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涓闄㈢寤虹墿璐ㄧ粨鏋勭爺絀舵墍楂橀箯鐮旂┒鍛樿棰樼粍鍦ㄦ潗鏂欓鍩熼《綰ф湡鍒?/span>銆?/span>Advanced Materials銆?/span>涓婂彂琛ㄤ簡棰樹負(fù)鈥?/span>Marked Passivation Effect of Naphthalene-1,8-Dicarboximides in High-Performance Perovskite Solar Cells鈥?/span>鐨勬枃绔狅紙DOI: 10.1002/adma.202008405錛夈傛敼鏂囩珷鐨勭涓浣滆呬負(fù)涓闄㈢寤虹墿璐ㄧ粨鏋勭爺絀舵墍涓庣宸炲ぇ瀛︾殑鑱斿悎鍩瑰吇紜曞＋鐢熷紶蹇楃殦錛岄珮楣忕爺絀跺憳涓烘湰鏂囩殑閫氳浣滆呫傚叾涓悊璁鴻綆楅儴鍒嗗緱鍒頒簡鍖椾含甯堣寖澶у榫欓棸鏁欐巿鍥㈤槦鐨勬敮鎸併?/span>


緙洪櫡閽濆寲鏄彁鍗囬挋閽涚熆澶槼鑳界數(shù)姹犲厜鐢?shù)铦{鎹㈡晥鐜囦笌紼沖畾鎬ф渶鏈夋晥鐨勬柟娉曘傝礬鏄撴柉紕辨槸閽欓挍鐭垮お闃寵兘鐢墊睜鏈甯哥敤鐨勯挐鍖栨坊鍔犲墏涔嬩竴錛岃瀹氫箟鍏鋒湁C=O銆?/span>S=O銆?/span>P=O銆?/span>-CN絳夊惛鐢?shù)瀛愬畼鑳藉洟鐨勬湁鏈簽畯鍒嗗瓙锛屾槸鑳藉缁欎簣澶栫晫鐢?shù)瀛愮殑鐢?shù)瀛愬渚涗綋銆傚湪浼犵粺鐨勮礬鏄撴柉紕變笂娣誨姞璐ㄥ瓙瀹樿兘鍥紙-OH銆?/span>-NH絳夛級(jí)鐨勫垎瀛愯櫧鐒舵樉紺哄嚭浜嗘瘮綰礬鏄撴柉紕辨洿楂樻晥鐨勯挐鍖栨晥鏋滐紝浣嗗叾璇︾粏鐨勪綔鐢ㄦ満鐞嗕粛鐒舵湭琚繁鍏ョ爺絀朵笌璇佹槑銆傚彟涓鏂歸潰錛岀悊璁鴻綆楀凡璇佹槑琛ㄩ潰媧繪ф哀錛堣秴姘х瀛?/span>O2-錛変細(xì)瀵歸挋閽涚熆钖勮啘涓庡櫒浠剁殑紼沖畾鎬ч犳垚鎹熷錛屼絾鏄洰鍓嶅嚑涔庢病鏈夐拡瀵歸闃茶秴姘ч檷瑙ｉ挋閽涚熆榪囩▼鐨勯挐鍖栧垎瀛愮殑鐩稿叧瀹為獙鐮旂┒銆?br />

鏈伐浣滃皢璺槗鏂⒈瀹樿兘鍥笌璐ㄥ瓙瀹樿兘鍥簬鑱氳姵棣欏叡杞垎瀛愪笂榪涜浜嗙粍鍚堬紝寰楀埌浜嗙函璺槗鏂⒈浣撶郴鍒嗗瓙9CN-PMI涓庤礬鏄撴柉紕?/span>/璐ㄥ瓙浣撶郴鍒嗗瓙4OH-NMI錛屽茍灝嗗叾寮曞叆鍒伴挋閽涚熆鍓嶉┍浣撴憾娑蹭腑錛屽埗澶囧緱鍒頒簡閽濆寲涔嬪悗鐨勯挋閽涚熆钖勮啘涓庡櫒浠躲傞氳繃瀵逛袱縐嶄笉鍚岀被鍨嬪垎瀛愮殑琛ㄥ緛瀵規(guī)瘮錛岃瘉鏄庝簡鍏鋒湁璺槗鏂⒈/鑱氳姵棣欏叡杞?/span>/璐ㄥ瓙緇撴瀯鐨勫垎瀛?/span>4OH-NMI鑳藉璧峰埌鏇村姞浼樺紓鐨勫寲瀛﹂挐鍖栵紙Chemical passivation錛変綔鐢紝鍏舵墍鎷ユ湁鐨?/span>C=O/-OH瀹樿兘鍥綋緋諱笉浠呰兘澶熸湁鏁堥挐鍖栨璐熺數(shù)鑽風(fēng)己闄蜂笌閾呭洟綈囷紝閽濆寲鍓傜殑-OH鍙互閫氳繃姘㈤敭涓?/span>I-鐩鎬簰浣滅敤錛屼粠鑰屼績榪?/span>C=O鍩哄洟涓庡弽浣?/span>Pb2 緙洪櫡鐨勭浉浜掔粨鍚堬紝浣垮緱閽濆寲鏁堟灉鏈澶у寲銆備笌姝ゅ悓鏃訛紝鏈枃閫氳繃鐞嗚璁＄畻涓庣ǔ瀹氭ф祴璇曪紝璇佹槑浜?/span>4OH-NMI鍏鋒湁鏇村姞鏄捐憲鐨勮兘甯﹂挐鍖栵紙Energetic passivation錛変綔鐢紝鍗抽挐鍖栧垎瀛愪駭鐢熻壇鎬х殑涓棿鑳介殭鎬侊紝璇ヨ兘闅欐佷綅浜?/span>O2浜х敓鐨勭數(shù)瀛愰櫡闃辨佷箣涓婏紝鑳藉鎶㈠湪O2涔嬪墠鎹曡幏閽欓挍鐭夸笂鐨勫厜嬋鍙戠數(shù)瀛愶紝閬垮厤瓚呮哀紱誨瓙鐨勫艦鎴愶紝榪涜屾彁楂橀挋閽涚熆鍣ㄤ歡鐨勭ǔ瀹氭с傛澶栵紝鏈枃鎰忓鍦板彂鐜?/span>4OH-NMI涓?/span>9CN-PMI鐨勫姞鍏ュ彲浠ユ彁楂橀挋閽涚熆鍓嶉┍浣撴憾娑茬殑綺樺害錛屼粠鑰屾樉鐫澧炲姞閽欓挍鐭胯啘鐨勫帤搴︿互瀹炵幇鏇撮珮鐨勫厜鏀墮泦鏁堢巼銆傛渶緇?/span>4OH-NMI閽濆寲鍚庣殑閽欓挍鐭跨數(shù)姹犳晥鐜囬珮杈?/span>23.7%涓旇〃鐜板嚭浼樺紓鐨勭ǔ瀹氭с?/span>


鍥?. a錛?span style="font-family:Calibri;">4OH-NMI瀵歸挋閽涚熆涓悇綾葷己闄風(fēng)殑鍖栧閽濆寲鏁堟灉銆?span style="font-family:Calibri;">b錛夊墠椹變綋婧舵恫涓姞鍏?span style="font-family:Calibri;">4OH-NMI鍚庯紝澧炲姞浜嗚杽鑶滅殑綺樺害錛屼嬌鑶滃帤澧炲姞錛岃杽鑶滆川閲忔彁楂橈紙綺樺害鐩稿叧琛ㄥ緛瑙?span style="font-family:Calibri;">SI錛夈?/span>


鍥?. a錛?4OH-NMI鍜?span style="font-family:Calibri;">9CN-PMI鐨勮〃闈㈤潤鐢?shù)鍔垮垎甯冨浘銆?span style="font-family:Calibri;">b錛?4OH-NMI/DMF銆?span style="font-family:Calibri;">9CN-PMI/DMF銆?span style="font-family:Calibri;">4OH-NMI/PbI2/DMF鍜?span style="font-family:Calibri;">9CN-PMI-PbI2/DMF婧舵恫鐨勭傳澶?span style="font-family:Calibri;">-鍙鍚告敹鍏夎氨銆?span style="font-family:Calibri;">c- d錛夊尯鍩熸斁澶х殑FTIR鍏夎氨錛?span style="font-family:Calibri;">c錛?span style="font-family:Calibri;">4OH-NMI綺夋湯鍜?span style="font-family:Calibri;">4OH-NMI/PbI2綺夋湯錛宒錛?span style="font-family:Calibri;">9CN-PMI綺夋湯鍜?span style="font-family:Calibri;">9CN-PMI/PbI2綺夋湯銆傚弬姣旇杽鑶溿?CN-PMI閽濆寲钖勮啘鍜?span style="font-family:Calibri;">4OH-NMI閽濆寲钖勮啘鐨?/span>O 1s錛?span style="font-family:Calibri;">e錛夈?/span>Pb 4f錛?span style="font-family:Calibri;">f錛夊拰I 3d錛?span style="font-family:Calibri;">g錛夊嘲鐨?span style="font-family:Calibri;">XPS璋便?/span>


鍥?. 錛坅-c錛?span style="font-family:Calibri;">4OH-NMI閽濆寲鍣ㄤ歡鍜屽弬姣斿櫒浠剁殑鐑綰沖厜璋辯浉鍏蟲祴璇曪紙TAS錛夛細(xì)a錛?鑾壒-鑲栫壒鍩哄浘錛?span style="font-family:Calibri;">b錛夌數(shù)瀹?span style="font-family:Calibri;">-棰戠巼鍏崇郴鍥撅紝c錛夎綆楀緱鍒扮殑闄烽槺鎬佸瘑搴︼紙NT錛夈俤錛?ss-PL鍏夎氨錛堥挋閽涚熆/FTO/鐜葷拑錛夛紝e錛?span style="font-family:Calibri;">tr-PL鍏夎氨錛堥挋閽涚熆/SiO2鐜葷拑錛夛紝f錛?span style="font-family:Calibri;">XRD鍥捐氨銆傦紙g-i錛夊悇縐嶇被钖勮啘鐨勬壂鎻忕數(shù)瀛愭樉寰暅錛?span style="font-family:Calibri;">SEM錛夊浘鐗囷紝姣斾緥灝?span style="font-family:Calibri;">2 mM銆?/span>


鍥?/span>4. a錛?鍙傛瘮鍣ㄤ歡涓?span style="font-family:Calibri;">4OH-NMI閽濆寲鍣ㄤ歡鐨凧-V鏇茬嚎錛?span style="font-family:Calibri;">b錛変笂榪頒袱縐嶅櫒浠剁殑鏈澶у姛鐜囩偣鐨勭ǔ瀹氭渶澶у姛鐜囪緭鍑猴紙鍙傛瘮鍣ㄤ歡涓?span style="font-family:Calibri;">0.92 V錛?span style="font-family:Calibri;">4OH-NMI閽濆寲鍣ㄤ歡涓?span style="font-family:Calibri;">1.01 V錛夛紝c錛?span style="font-family:Calibri;">PCE鍒嗗竷緇熻鍥撅紝 d錛?span style="font-family:Calibri;">EQE鍏夎氨銆?span style="font-family:Calibri;">e錛夋湁鏁堥潰縐負(fù)1 cm2鐨勫弬姣斿櫒浠跺拰4OH NMI閽濆寲鍣ㄤ歡鐨勫弽鎵?span style="font-family:Calibri;">J-V鏇茬嚎銆?span style="font-family:Calibri;">f錛夋湁鏁堥潰縐負(fù)1 cm2鐨勭數(shù)姹犵収鐗囥?/span>


鍥?. a-b錛?span style="font-family:Calibri;">4OH NMI閽濆寲鍣ㄤ歡銆?span style="font-family:Calibri;">9CN PMI閽濆寲鍣ㄤ歡銆佷笌鍙傛瘮鍣ㄤ歡鐨勭ǔ瀹氭ц瘯楠岋細(xì)a錛夊湪N2姘旀皼涓殑闀挎湡紼沖畾鎬э紱b錛?鍦ㄦ哀姘斾笌鐩稿婀垮害涓?span style="font-family:Calibri;">20-30% RH鐨勭幆澧冧腑鐨勭ǔ瀹氭э紝嫻嬭瘯娓╁害涓?5鈩冿紱閽欓挍鐭垮湪錛坅錛?span style="font-family:Calibri;">4OH-NMI鍜岋紙b錛?CN-PMI閽濆寲涓斿惛闄?span style="font-family:Calibri;">O2鎯呭喌涓嬬殑鑷棆鎶曞獎(jiǎng)鎬佸瘑搴︺傚垎瀛愪駭鐢熺殑涓棿鑳介殭鎬侀珮浜庢哀姘斾駭鐢熺殑闄烽槺鎬侊紝鏈夊埄浜庢崟鑾烽挋閽涚熆鍏夋縺鍙戠數(shù)瀛愬茍鎶戝埗瓚呮哀紱誨瓙鐨勫艦鎴愩?/span>


  鏈珷鐨勫伐浣滀負(fù)澶氬姛鑳介挐鍖栧垎瀛愮殑璁捐鎻愪緵浜嗘柊鐨勬濊礬錛氾紙1錛夊垎瀛愪腑璺槗鏂⒈瀹樿兘鍥紙C=O銆?/span>S=O銆?/span>P=O銆?/span>-CN錛夊拰璐ㄥ瓙瀹樿兘鍥紙-OH銆?/span>-NH銆?SH錛夌殑緇勫悎鏄疄鐜伴挋閽涚熆钖勮啘娣辮兘綰т笌嫻呰兘綰х己闄烽珮鏁堥挐鍖栫殑鍏抽敭錛涳紙2錛夋帹鎷夊瀷鐢?shù)瀛惥l撴瀯涓嶄粎鎻愪緵浜嗗己鍋舵瀬鐭╋紝鑰屼笖澧炲姞浜嗛潪緇濈儹鐢?shù)瀛?/span>-澹板瓙鑰﹀悎錛涳紙3錛夊叿鏈夎礬鏄撴柉紕?/span>/鑱氳姵棣欏叡杞?/span>/璐ㄥ瓙浣撶郴鐨勫垎瀛愯兘澶熻皟鑺傞挋閽涚熆灞傚帤搴︼紝鍥犳鏋佹湁娼滃姏浠ュ簲鐢ㄤ簬涓ょ鍙犲眰閽欓挍鐭垮お闃寵兘鐢墊睜錛屼互瀹炵幇鏇村ソ鐨勭數(shù)嫻佸尮閰嶏紱錛?錛夐傚綋璁捐鐨?/span>p浣撶郴鍒嗗瓙鑳藉浜х敓涓棿鑳介殭鎬佷簬O2浜х敓鐨勭數(shù)瀛愰櫡闃辨佷箣涓婏紝鎶㈠ず鍏夋縺鍙戠數(shù)瀛愬茍鎶戝埗瓚呮哀紱誨瓙鐢熸垚銆?/span>


楂橀箯璇鵑緇勭綉绔?/span>

https://www.x-mol.com/groups/gao_peng


鐩稿叧閾炬帴

https://onlinelibrary.wiley.com/doi/10.1002/adma.202008405

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